Certified methods developed in 2001 — 2015

№ of calibration certificate Document for MM Measurement range
Analytical control of amine treating processes and elemental sulfur production
1 65606-04 of 23.08.2004

FR.1.31.2005.01509

Volume fraction of components. Sour gases of effluent stripping (CO2, H2S, NH3) 0.1 % — 50.00 %
2 68606-04 of  25.08.2004

FR.1.31.2005.01508

Volume fraction of H2S, CO2 and Н2. Process gas 0.02 % — 10.00 %
3 68806-04 оf 25.08.2004

FR.1.31.2005.01506

Volume fraction of components. Process gas (N2, CO2, H2S и SO2). 0,02 % — 70,00 %
4 68706-04 оf 25.08.2004

FR 1.31.2005.01507

Volume fraction of CO2, H2S и Н2О. Process gas. 0,3 % — 80,00 %
5 68906-04 оf 28.08.2004

FR.1.31.2005.01505

Volume fraction of components. Sour gases of amine regeneration (CO2, H2S, NH3, Н2О and С15 hydrocarbons)

H2S- main component..

0,1 % — 3,00 %
6 1459-06 от 23.11.2006 Sour gases of amine regeneration of elemental sulfur production plant. Volume fraction of components (CO2, H2S, NH3, Н2О and С15 hydrocarbons).

H2S- main component +mercaptans.

0,01 % — 3,00 %

10 ppm — 500 ppm

7 1559-06 от 23.11.2006 Aqueous amine solutions and wash waters. DEA mass fraction. 0,3 — 4,0 %

20,0 % — 35,0 %

8 1659-06 от 23.11.2006 Sour gases of effluent stripping. Volume fractions of components (CO2, H2S, NH3  and С15 hydrocarbons). 0.05 % — 50.00 %

10 ppm — 500 ppm

9 89706-08 оf 28.05.2008 Aqueous amine solutions and sparging water. Mass fraction of CO2, H2S and NH3. МM 0,01 — 5,00 %
10 137806-08 оf 24.06.2008 Aqueous amine solutions and wash waters. Determination of mass fraction of MEA. МM 0,1 — 0,3 %

10,0 % -20,0 %

11 7606-09 оf 02.07.2009 State system of ensuring the uniformity of measurement. Aqueous amine solutions. Mass fraction of С15 hydrocarbons. МM 0,003 — 1,00 %
12 11106-09 оf 25.07.2009 Sour gas of amine regeneration. Volume fraction of components. МM 0.01 % — 10.00 %

75.00 % — 95.00 %

13 24806-09 оf 21.12.2009 Sour gases of effluent stripping. Determination of CO2, NH3, H2S and С15 hydrocarbons. МM 0.05 % — 50.00 %

20 mg/m3 — 1000 mg/m3.

14 65706-04 оf 23.08.2004

FR..1.31.2005.01510

Mass fraction of hydrogen sulfide, ammonia and carbon dioxide. Rich and regenerated solutions of МEА and МDEА 0.1 – 5.0 МEА

1.0 – 30.0 МDEА

Analysis of light hydrocarbon fractions
15 99906-01 оf 29.11.2001 МM of mass fraction of methanol in a wide fraction of light hydrocarbons by GC method 0,003 % — 0,3 % and higher
16 100006-01 оf 29.11.2001 МM of mass fraction of components in a wide fraction of light hydrocarbons by GC method 0,3 % — 30,0 % and higher
17 40106-02 оf 28.06.2002 МM of mass fraction of CO2 in ethane fraction  by GC method.

 

0.003 % — 0.03 %
18 40606-02 оf 28.06.2002 МM of mass fraction of water in associated oil gas by GC method 0.3 % — 3.0 %
19 42006-04 without date Volume fraction of components. Stabilization and flash gases 0.3 % — 30.0 % and higher
20 182406-07 1оf 8.08.2007 Hydrocarbon gas. Mass fraction of С24 hydrocarbons 0.1 – 60.0 %
21 144206-08 от 28.07.2008 Gas-air mixture in void spaces of compressor oil boxes. Volume fractions of hydrocarbon components 0.1 – 80.0 %
22 (98606-07)оf 30.05.2007

16806-13 оf 13.09.2013

Ethane fraction. GC method of component composition determination 0.001% — 3.5 % (mass)
23 11206-09 оf 25.07.2009 Ethane fraction. Mass fraction of СО2 0.003 – 1.00 %
24 4406-10 оf 25.02.2010 Flare gas from hydrogen-flare system. Volume fraction of components. МM  of (Н2, Н2S, NH3 and С1hydrocarbons) 0.30 – 90.00 %
25 01.00257-2008/18706-11

оf 13.12.2011

FR..1.29.2011.11468

Heating gas. GC method of component composition determination. (Н2, О2, N2,CO, CO2, H2S) 0.10 – 85.00 %

0.5g/m3  — 15.0 g/m3

26 29306-12 от 29.10.12

FR..1.31.2013.14306

(42006-04) without date

Volume fraction of components. Stabilization and flash gases 0.01 % — 70.0 %

0.3 — 30 and higher

27 01.00257-2008/4006-13

от 02.04.2013

FR..1.31.2014

17506-10 оf 15.09.2010

Ethanated wide fraction of light hydrocarbons. Mass fraction of СО2. МM. 0.010 – 3.00 %

 

0.1-3

28 01.00257-2013/28606-15

оf 19.10.2015

MM of mass fraction of С16 hydrocarbons and methanol in wide fraction of light hydrocarbons. 0.010 – 50.000 %
29 01.00257-2008/25406-13

оf 29.11.2013

FR.1.31.2014.18560

Associated oil gas. Determination of component composition by GC method. 0,001 — 95,000 mole fr., %
30 36806 оf

3 December 2015

Sour gas. Determination of mole fraction of components by GC method. 0.01 – 80.00 %
31 36706 оf

3 December 2015

Associated oil gas. Determination of volume fraction of water by GC method. 0.03 – 4.00 %
Determination of sulfur-containing compounds
32 170806-07 оf 30.06.2007 Spent air of alkaline solution regeneration unit. Mass fraction of dialkyl disulfides. MM 0.03 – 10.00 %
33 20506-07 оf 26.02.2007

FR.1.31.2015.19926

Disulfide oil. Mass fraction of dialkyl disulfides. 0.1 – 95.0 %
34 157106-08 оf 14.06.2008

 

Hydrocarbon solvent. Mass fraction of dialkyl disulfides. МM 0.01 – 60.0 %
35 7506-09 оf 02.07.2009

FR.1.31.2015.19932

Purified associated oil gas. Mass fraction of sulfur-containing compounds.МM. 3 mg/m3 — 1000 mg/m3
36 29306-09 оf 15.12.2009

FR.1.31.2015.19929

State system of ensuring the uniformity of measurement. Liquefied hydrocarbon gases. Mass fraction of sulfur-containing compounds. .0.0003 % — 0.1000 %..
37 01.00257-2008/22906-12

оf 31.08.2012

FR.1.31.2013.14307

Light gasoline fraction. Determination of mass fraction of sulfur-containing compounds by GC method. МM. 1-100 ррм mass of elemental sulfur
Non-hydrocarbon gases
38 01.00257-2008/18806-11

оf 13.12.2011

Argon fraction. Determination of volume fraction of oxygen by GC method. МИ. 0.10 – 50.00 %
39 01.00257-2008/13306-11

оf 27.09.2011

Industrial gaseous oxygen. Determination of impurities content by GC method (Ar, He, H2, CH4, N2, CO and СО2) 0.01 – 1.00 % vol.

1.0 mg/m3  — 50.0 mg/m3

40 01.00257-2008/38806-12

оf 27.12.2012

FR.1.31.2014

Liquefied oxygen. Determination of volume fraction of oxygen, argon, nitrogen. Oxygen  60.00 —  99.90

argon 0.10 – 10.00 %   nitrogen  0.10 – 40.00 %

41 01.00257-2008/32506-12

оf

FR.1.31.2013.14329

Liquid air. Determination of volume fraction of oxygen, argon, nitrogen argon 0.5 % — 10 %

oxygen  20.0 % —  40.0 %

nitrogen   50 % — 80 %

42 01.00257-2013/26506-14

replaced оn  26.12.2014

Liquefied oxygen. Determination of oil content by GC method. МM  0.010 – 5.000 mg/dm3

( 0.050 – 5.000 mg/dm3)

43 01.00257-2008/30706-13

оf 26.07.2013

Liquid air. Determination of carbon dioxide by GC method. МM.  0.10 – 5.00 сm3/dm3
Federal environmental regulatory documents
44 PND F 13.1:2.22-98 Determination of volume fraction of Н2, О2, N2, CH4, CO and CO2 in occupational air and industrial emissions. 0.1 – 90.0 % vol.
45 PND F 13.1:2:3.23-98

Fr.1.31.2015.20483

Determination of mass concentration of saturated С15 hydrocarbons and non-saturated hydrocarbons (ethene, propene, butenes) in occupational air and industrial emissions. 1 — 1500 mg/m3
46 PND F 13.1:2:3.24-98 Determination of mass concentration of hexane, heptane, оctane, nonane and decane in atmospheric air, occupational air and industrial emissions. 1.0 — 1000 mg/m3
47 PND F 13.1:2:3.25-99

Fr.1.31.2015.20480

Determination of mass concentration of saturated С110 hydrocarbons (in total, calculated as carbon), non-saturated С25 hydrocarbons (in total, calculated as carbon) and aromatic hydrocarbons (benzene, toluene, ethyl benzene, xylenes, styrene) at their joint presence in atmospheric air, occupational air and industrial emissions. 0.2 — 1000 mg/m3
48 PND F 13.1:2.26-99

Fr.1.31.2015.20478

Determination of mass concentration of saturated С15, С6 hydrocarbons and higher (in total) in occupational air and industrial emissions. 1 — 1500 mg/m3
49 PND F 13.1:2:3.27-99

Fr.1.31.2015.20481

Determination of mass concentration of carbon oxide and methane in atmospheric air, occupational air and industrial emissions by reaction GC method. 2 — 600 mg/m3
The rest
50 209806-07 оf 23.10.2007

 

Non-stable gas condensate. Density measurement method 600 kg/m3 — 800  kg/m3
51 89606-08 оf 28.03.2008 Catalyst. Мass fraction of coke.  0.01 – 2.00 %
52 01.00257-2008/27606-10 оf 25.10.2010 Non-stable gas condensate. Density measurement method. 500 kg/m3 — 900  kg/m3
53 01.00257-2008/39006-12

оf 27.12.2012

Fr.1.31.2014

Water-methanol mixture. Mass fraction of methanol in water-methanol mixture. 0.10 % — 3.00 %

 

Our methods

List of methods developed by OJS “VNIIUS”

  • Aqueous amine solutions and sparging water. Mass fraction of CO2, H2S and NH3. MM. Calibration certificate № 89706-08 оf 28.05.08.
  • Aqueous amine solutions and washing waters. Mass fraction of DEA. MM. Calibration certificate № 1559-06 оf 23.11.06.
  • Aqueous amine solutions and washing waters. Determination of mass fraction of MEA. MM. Calibration certificate № 137806 – 08 оf 24.06.08.
  • State system for ensuring the uniformity of measurements. Aqueous amine solutions. Mass fraction of С15 hydrocarbons. MM. Calibration certificate № 7606-09 оf 02.07.09.
  • Gasoline light fraction. Determination of mass fraction of sulfur-containing compounds by GC method. М Calibration certificate № 01.00257 – 2008/22906 — 12 оf 31.08.12.
  • Non-stable gas condensate. Method of density measurement. Calibration certificate № 27606 — 10 оf 25.10.10.
  • Spent air of alkaline solution regeneration unit. Mass fraction of dialkyl disulfides. MM. Calibration certificate № 170806 — 07 оf06.07.
  • Disulfide oil. Mass fraction of dialkyl disulfides. MM. Calibration certificate № 20506-07 оf 26.02.07.
  • Non-stable gas condensate. Method of density measurement. Calibration certificate № 209806-07 оf10.07.
  • Мass fraction of coke. MM. Calibration certificate № 89606-08 оf 28.03.08.
  • Treated associated petroleum gas. Mass concentration of sulfur-containing compounds. MM. Calibration certificate № 7506-09 оf 02.07.09.
  • Method of measurement of mass fraction of methanol in a wide fraction of light hydrocarbons using chromatography. MM. Calibration certificate № 99906-01 оf 29.11.01.
  • Hydrocarbon solvent. Mass fraction of dialkyl disulfides. MM. Calibration certificate № 157106-08 оf 06.08.
  • Gas-air mixture in void spaces of compressor oil boxes. Volume fractions of hydrocarbon components. MM. Calibration certificate № 144206.
  • Sour gases of effluents steaming. Volume fractions of components. (CO2, H2S, NH3and С15 hydrocarbons). MM. Calibration certificate № 1659-06 оf 23.11.06.
  • Flare gas from hydrogen-flare system. Volume fractions of components. МM (Н2, Н2S, NH3, С15 hydrocarbons). MM. Calibration certificate № 4406-10 оf 25.02.10.
  • Sour gases of effluents steaming. Determination of CO2, NH3, H2S, and С1-С MM. Calibration certificate № 24806-09 оf 24.12.09.
  • Volume fraction of components. Technologic gas (N2, CO2, H2S and SO2). MM. Calibration certificate № 68806 – 04 оf 25.08.04.
  • Ethane fraction. Chromatographic method of component composition determination. MM. Calibration certificate № 98606 – 07 оf 30.05.07.
  • Volume fraction of CO2, H2S and Н2О. Technologic gas. MM. Calibration certificate № 68706 – 04 оf 25.08.04.
  • Sour gases of amine regeneration plants producing elemental sulfur. Volume fractions of components (CO2, H2S, NH3,, Н2О and С15 hydrocarbons). MM. Calibration certificate № 1459 – 06 оf 23.11.06.
  • Volume fraction of components. Sour gases of effluents steaming (CO2, H2S, NH3). MM. Calibration certificate № 65606 — 04 оf 23.08.04.
  • MM of mass fraction of components in a wide fraction of light hydrocarbons using chromatography. MM. Calibration certificate № 100006-01 оf11.01.
  • Heating gas. Determination of component composition by GC method. М (Н2, О2, N2,CO, CO2, H2S). Calibration certificate № 18706-11 оf 13.12.11.
  • Ethanated wide fraction of light hydrocarbons. Mass fraction of СО. М Calibration certificate № 01.00257-2008/4006-13.
  • Hydrocarbon gas. Mass fraction of С24 MM. Calibration certificate № 182406-07 оf 28.08.07.
  • Argon fraction. Determination of volume fraction of oxygen by GC method. М Calibration certificate № 18806-11 оf 13.12.11.
  • Volume fraction of components. Stabilization and flash gases. MM. Calibration certificate № 29306-12 оf 29.10.12.
  • Industrial gas oxygen. Determination of impurities content by GC method (Ar, He, H2, CH4, N2, CO and СО2). М Calibration certificate № 01.00257—2008/13306-11 оf 27.09.11.
  • Volume fraction of components. Sour gases of amine regeneration (CO2, H2S, NH3,Н2О and С15 hydrocarbons). MM. Calibration certificate №68906 – 04 оf 25.08.2004.
  • Volume fraction of H2S, CO2, and Н2. Technologic gas. MM. Calibration certificate № 68606 – 04 оf 25.10.2004.
  • Sour gas of amine regeneration. Volume fraction of components. MM. Certificate № 11106 — 09 25 оf July 2009.
  • Liquid air. Determination of volume fraction of argon, oxygen, nitrogen. MM. Certificate № 01.00257 — 2008/32506 – 12.
  • Liquid oxygen. Determination of volume fraction of argon, oxygen, nitrogen. MM. Calibration certificate № 01.00257—2008/38806—12 оf 27.12.12.
  • Water-methanol mixture. Mass fraction of methanol in water-methanol mixture. М Calibration certificate of measurement method № 01.00257—2008/39006—12 оf 27.12.12.
  • Liquid oxygen. Determination of oil content by GC method. М Calibration certificate of measurement method №01.00257–2013/25406–14.
  • Associated petroleum gas. Determination of component composition by GC method. МИ. Calibration certificate of measurement method №01.00257—2008/25406—13.
  • Liquid air. Determination of carbon dioxide by GC method. М Calibration certificate of measurement method № 01.00257–2008/ 30706–13.